DIKEGULAC DIHYDRAT
- CAS NO.：18467-77-1
- Empirical Formula: C12H18O7
- Molecular Weight: 274.27
- MDL number: MFCD00150519
- EINECS: 242-348-8
- SAFETY DATA SHEET (SDS)
- Update Date: 2024-12-18 13:37:16
What is DIKEGULAC DIHYDRAT?
Definition
ChEBI: Dikegulac is a member of dioxanes.
Purification Methods
Dissolve -DAG in Et2O, filter, dry (MgSO4) it, filter it again and evaporate to give a yellow oil. Addition of one drop of H2O induces crystallisation to the monohydrate, which also forms rhombic crystals on recrystallisation from 95% EtOH/H2O at room temperature. [Flatt et al. Synthesis 815 1979, Reichstein & Grussner Helv Chim Acta 17 311 1934, Takagi & Jeffrey Acta Crystallogr Sect B 34 2932 1978, cf Org Synth 55 80 1976, Beilstein 19/12 V 520.]
Properties of DIKEGULAC DIHYDRAT
| Melting point: | 88-90 °C(lit.) |
| Boiling point: | 375℃ |
| Density | 1.281 |
| Flash point: | 140℃ |
| storage temp. | 2-8°C |
| pka | 1.77±0.60(Predicted) |
| EPA Substance Registry System | .alpha.-L-xylo-2-Hexulofuranosonic acid, 2,3:4,6-bis-O-(1-methylethylidene)- (18467-77-1) |
Safety information for DIKEGULAC DIHYDRAT
Computed Descriptors for DIKEGULAC DIHYDRAT
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