Palladium (II) Acetate
Synonym(s):Palladium diacetate;Palladium(II) acetate;Palladium(II) acetate (47% Pd);Palladium(II) acetate impregnated tablets;Pd(OAc)2
- CAS NO.:3375-31-3
- Empirical Formula: Pd(OCOCH3)2
- Molecular Weight: 226.52
- MDL number: MFCD00012453
- EINECS: 222-164-4
- SAFETY DATA SHEET (SDS)
- Update Date: 2024-05-06 14:33:24
What is Palladium (II) Acetate?
The Uses of Palladium (II) Acetate
Palladium (II) Acetate Trimer is used in Suzuki-Miyaura cross-coupling reactions. It also serves to catalyze the chemoselective reduction of nitroarenes.
The Uses of Palladium (II) Acetate
The Iodo compound (308 mg, 0.513 mmol), the boronic ester (194 mg, 0.641 mmol), K3PO4 (327 mg, 1.539 mmol), XPhos (14.67 mg, 0.031 mmol), and Pd2(dba)3 (14.09 mg, 0.015 mmol) were combined in a microwave vial. The vial was purged with argon, after which time was added dioxane (3 mL) and H2O (0.5 mL) The reaction was irradiated in a microwave reactor at 120 C for 10 min. Additional boronic ester (50 mg) was added and the mixture was irradiated at 120 C for another 10 min. The mixture was then treated with aq 1N NaOH and extracted with EtOAc (50 mL). The org layer was dried (MgSO4), concentrated, and purified by flash chromatography (20% MeOH/DCM) to provide the product as a dark yellow solid. [177 mg, 53%]
What are the applications of Application
Palladium(II) acetate is a catalyst for intramolecular coupling
Properties of Palladium (II) Acetate
Melting point: | 205 °C |
storage temp. | Store below +30°C. |
solubility | Soluble as monomer in glacial acetic acid or as trimer in benzene. |
form | Various Forms In Red-(Powder/Flake/Crystalline/Beads) |
appearance | Brown/orange solid |
color | Red-brown |
Water Solubility | insoluble |
Sensitive | Hygroscopic |
Safety information for Palladium (II) Acetate
Signal word | Danger |
Pictogram(s) |
Corrosion Corrosives GHS05 Exclamation Mark Irritant GHS07 Environment GHS09 |
GHS Hazard Statements |
H317:Sensitisation, Skin H318:Serious eye damage/eye irritation H410:Hazardous to the aquatic environment, long-term hazard |
Precautionary Statement Codes |
P261:Avoid breathing dust/fume/gas/mist/vapours/spray. P272:Contaminated work clothing should not be allowed out of the workplace. P273:Avoid release to the environment. P280:Wear protective gloves/protective clothing/eye protection/face protection. P302+P352:IF ON SKIN: wash with plenty of soap and water. P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing. |
Computed Descriptors for Palladium (II) Acetate
InChIKey | PCUVQHHZCJMCHO-UHFFFAOYSA-M |
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