Ethyl 3-Amino-4-methylbenzoate
- CAS NO.：41191-92-8
- Empirical Formula: C10H13NO2
- Molecular Weight: 179.22
- MDL number: MFCD01926538
- SAFETY DATA SHEET (SDS)
- Update Date: 2026-05-28 03:02:39
What is Ethyl 3-Amino-4-methylbenzoate?
Synthesis
Dissolve 10 g of palladium on carbon (10%) and 140 g of ammonium formate in 400 ml of methanol, and then dissolve 136 g of ethyl 3-nitro-4-methylbenzoate (2) in 400 ml of methanol. Add the methanol solution of (2) dropwise to the reaction flask at room temperature. The reaction exotherms until the methanol boils. Continue the dropwise addition. After the dropwise addition, TLC detects the completion of the reaction and filters the palladium carbon. Concentrate the methanol, add 400ml of water, and filter to obtain 156g of white solid ethyl 3-amino-4-methylbenzoate (Ethyl 3-Amino-4-methylbenzoate) as a wet product, which can be used in the next step without drying.
Properties of Ethyl 3-Amino-4-methylbenzoate
| Melting point: | 48.6-50.1℃ |
| Boiling point: | 105°C/0.2mmHg(lit.) |
| Density | 1.103±0.06 g/cm3(Predicted) |
| storage temp. | under inert gas (nitrogen or Argon) at 2–8 °C |
| solubility | soluble in Methanol |
| form | powder to crystal |
| pka | 3.35±0.10(Predicted) |
| color | White to Almost white |
Safety information for Ethyl 3-Amino-4-methylbenzoate
| Signal word | Warning |
| Pictogram(s) |
 Exclamation Mark Irritant GHS07 |
| GHS Hazard Statements |
H315:Skin corrosion/irritation H319:Serious eye damage/eye irritation |
| Precautionary Statement Codes |
P264:Wash hands thoroughly after handling. P264:Wash skin thouroughly after handling. P280:Wear protective gloves/protective clothing/eye protection/face protection. |
Computed Descriptors for Ethyl 3-Amino-4-methylbenzoate
| InChIKey | MCNBNDUVWQEKNZ-UHFFFAOYSA-N |
New Products
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